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1. Development of a grignard-type reaction for manufacturing in a continuous-flow reactor
Odille, Fabrice
et al.

RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Process Development, Processutveckling och kristallisation. AstraZeneca, Sweden.

Stenemyr, Anna
RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Process Development, Processutveckling och kristallisation. AstraZeneca, Sweden.
Ponten, Fritiof
AstraZeneca, Sweden.
Development of a grignard-type reaction for manufacturing in a continuous-flow reactor2014In: International journal of thermophysics, ISSN 0195-928X, E-ISSN 1572-9567, Vol. 18, no 11, p. 1545-1549Article in journal (Refereed)
Abstract [en]
This paper describes the scale-up of a highly exothermic and fast reaction from a microreactor with an internal volume of less than 1 mL to a mesoreactor with an internal volume of 13.5 mL. The development of a continuous process for manufacturing a ketone from an ester using a Grignard reagent is described. The different steps undertaken and the considerations made to be able to operate in continuous mode and achieve a product output of ca. 0.5 kg are presented.
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