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  • 1. Andersson, Nina
    et al.
    Corkery, Robert W
    YKI – Ytkemiska institutet.
    Alberius, Peter CA
    YKI – Ytkemiska institutet.
    One-pot synthesis of well ordered mesoporous magnetic carriers2007In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 17, no 26, p. 2700-2705Article in journal (Refereed)
    Abstract [en]

    The facile preparation of a mesoporous magnetic carrier technology is demonstrated. The micron-sized spherical mesostructured particles are prepared using a newly-developed, one-step, combined emulsion and solvent evaporation (ESE) method. The surfactant-templated silica matrix display a well-ordered internal pore architecture. Very limited pore blocking, and only to a limited degree disordered- or worm-like structures are observed, induced by the iron oxide nanoparticles added to provide the superparamagnetic properties.The iron oxide content was precisely controlled, and the magnetic properties were well preserved during the process. Finally we demonstrate the applicability of the magnetically separable mesoporous material as an adsorbent for specific dissolved materials from dilute aqueous solutions.

  • 2.
    Bamgbopa, Musbaudeen
    et al.
    Linköping University, Sweden.
    Edberg, Jesper
    RISE - Research Institutes of Sweden, ICT, Acreo.
    Engquist, Isak
    Linköping University, Sweden.
    Berggren, Magnus
    Linköping University, Sweden.
    Tybrandt, Klas
    Linköping University, Sweden.
    Understanding the characteristics of conducting polymer-redox biopolymer supercapacitors2019In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 7, no 41, p. 23973-23980Article in journal (Refereed)
    Abstract [en]

    The growth of renewable energy production has sparked a huge demand for cheap and large-scale electrical storage solutions. Organic supercapacitors and batteries are envisioned as one, among several, candidates for this task due to the great abundance of their constituent materials. In particular, the class of supercapacitors based on conjugated polymer-redox biopolymer composites are of great interest, since they combine the benefit of high electrical conductivity of the conducting polymers with the low cost and high specific capacitance of redox biopolymers. The optimization of such complex systems is a grand challenge and until now there have been a lack of models available to ease that task. Here, we present a novel model that combines the charge transport and impedance properties of conducting polymers with the electrochemical characteristics of redox polymers. The model reproduces a wide range of experimental data and elucidates the coupling of several critical processes within these supercapacitors, such as the double-layer capacitance, redox kinetics and dissolution/release of the redox polymer to the electrolyte. Further, the model also predicts the dependencies of the power and energy densities on the electrode composition. The developed model shows how organic supercapacitors can be analyzed beyond archetypical equivalent circuit models and thus constitutes a promising tool for further advancements and optimization within the field of research of green energy storage technology.

  • 3.
    Edberg, Jesper
    et al.
    RISE - Research Institutes of Sweden, ICT, Acreo. Linköping University, Sweden.
    Inganas, Olle
    Linköping University, Sweden.
    Engquist, Isak
    Linköping University, Sweden.
    Berggren, Magnus
    Linköping University, Sweden; Stellenbosch University, South Africa.
    Boosting the capacity of all-organic paper supercapacitors using wood derivatives2018In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 6, no 1, p. 145-152Article in journal (Refereed)
    Abstract [en]

    Printed and flexible organic electronics is a steadily expanding field of research and applications. One of the most attractive features of this technology is the possibility of large area and high throughput production to form low-cost electronics on different flexible substrates. With an increasing demand for sustainable energy production, low-cost and large volume technologies to store high-quality energy become equally important. These devices should be environmentally friendly with respect to their entire life cycle. Supercapacitors and batteries based on paper hold great promise for such applications due to the low cost and abundance of cellulose and other forest-derived components. We report a thick-film paper-supercapacitor system based on cellulose nanofibrils, the mixed ion-electron conducting polymer PEDOT: PSS and sulfonated lignin. We demonstrate that the introduction of sulfonated lignin into the cellulose-conducting polymer system increases the specific capacitance from 110 to 230 F g(-1) and the areal capacitance from 160 mF cm(-2) to 1 F cm(-2). By introducing lignosulfonate also into the electrolyte solution, equilibrium, with respect to the concentration of the redox molecule, was established between the electrode and the electrolyte, thus allowing us to perform beyond 700 charge/discharge cycles with no observed decrease in performance.

  • 4.
    Erlandsson, Johan
    et al.
    KTH Royal institute of technology, sweden.
    Pettersson, Torbjörn
    KTH Royal institute of technology, Sweden.
    Ingverud, Tobias
    KTH Royal institute of technology, Sweden.
    Granberg, Hjalmar
    RISE - Research Institutes of Sweden, Bioeconomy.
    Larsson, Per A.
    KTH Royal institute of technology, Sweden.
    Malkoch, Michael
    KTH Royal institute of technology, Sweden.
    Wågberg, Lars
    KTH Royal institute of technology, Sweden.
    On the mechanism behind freezing-induced chemical crosslinking in ice-templated cellulose nanofibril aerogels2018In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 6, no 40, p. 19371-19380Article in journal (Refereed)
    Abstract [en]

    The underlying mechanism related to freezing-induced crosslinking of aldehyde-containing cellulose nanofibrils (CNFs) has been investigated, and the critical parameters behind this process have been identified. The aldehydes introduced by periodate oxidation allows for formation of hemiacetal bonds between the CNFs provided the fibrils are in sufficiently close contact before the water is removed. This is achieved during the freezing process where the cellulose components are initially separated, and the growth of ice crystals forces the CNFs to come into contact in the thin lamellae between the ice crystals. The crosslinked 3-D structure of the CNFs can subsequently be dried under ambient conditions after solvent exchange and still maintain a remarkably low density of 35 kg m-3, i.e. a porosity greater than 98%. A lower critical amount of aldehydes, 0.6 mmol g-1, was found necessary in order to generate a crosslinked 3-D CNF structure of sufficient strength not to collapse during the ambient drying. The chemical stability of the 3-D structure can be further enhanced by converting the hemiacetals to acetals by treatment with an alcohol under acidic conditions.

  • 5.
    Jiao, Fei
    et al.
    Linköping University, Sweden.
    Naderi, Ali
    BillerudKorsnäs, Sweden.
    Zhao, Dan
    Linköping University, Sweden.
    Schlueter, Joshua
    University of Kentucky, USA.
    Shahi, Maryam
    University of Kentucky, USA.
    Sundström, Jonas
    RISE - Research Institutes of Sweden, Bioeconomy. RISE, Innventia.
    Granberg, Hjalmar
    RISE - Research Institutes of Sweden, Bioeconomy. RISE, Innventia.
    Edberg, Jesper
    Linköping University, Sweden.
    Ail, Ujwala
    Linköping University, Sweden.
    Brill, Joseph
    BillerudKorsnäs, Sweden.
    Lindström, Tom
    RISE - Research Institutes of Sweden, Bioeconomy. RISE, Innventia.
    Berggren, Magnus
    Linköping University, Sweden.
    Crispin, Xavier
    Linköping University, Sweden.
    Ionic thermoelectric paper2017In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 5, p. 16883-16888Article in journal (Refereed)
    Abstract [en]

    Ionic thermoelectric materials, for example, polyelectrolytes such as polystyrene sulfonate sodium (PSSNa),constitute a new class of materials which are attracting interest because of their large Seebeck coefficientand the possibility that they could be used in ionic thermoelectric SCs (ITESCs) and field effect transistors.However, pure polyelectrolyte membranes are not robust or flexible. In this paper, the preparation of ionicthermoelectric paper using a simple, scalable and cost-effective method is described. After a compositewas fabricated with nanofibrillated cellulose (NFC), the resulting NFC–PSSNa paper is flexible andmechanically robust, which is desirable if it is to be used in roll-to-roll processes. The robust NFC–PSSNa thermoelectric paper combines high ionic conductivity (9 mS cm1), high ionic Seebeckcoefficient (8.4 mV K1) and low thermal conductivity (0.75 W m1 K1) at 100% relative humidity,resulting in overall figure-of-merit of 0.025 at room temperature which is slightly better than that for thePSSNa alone. Fabricating a composite with cellulose enables flexibility and robustness and this is anadvance which will enable future scaling up the manufacturing of ITESCs, but also enables its use fornew applications for conformable thermoelectric devices and flexible electronics.

  • 6.
    Johansson Salazar-Sandoval, Eric
    RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Kemi Material och Ytor.
    Hybrid acrylic/CeO2 nanocomposites using hydrophilic, spherical and high aspect ratio CeO2 nanoparticles2014In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 2, no 47, p. 20280-20287Article in journal (Refereed)
  • 7.
    Löwenhielm, Peter
    RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Kemi Material och Ytor, Medicinteknik.
    UV initiated thiol-ene chemistry: A facile and modular synthetic methodology for the construction of functional 3D networks with tunable properties2013In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 1, no 44, p. 13732-13737Article in journal (Refereed)
  • 8.
    Mille, Christian B
    et al.
    RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Kemi Material och Ytor.
    Corkery, Robert W
    RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Kemi Material och Ytor.
    A structural and thermal conductivity study of highly porous, hierarchical polyhedral nanofoam shells made by condensing silica in microemulsion films on the surface of emulsified oil drops2013In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 1, no 5, p. 1849-1859Article in journal (Refereed)
    Abstract [en]

    Light-weight solid foams are utilized in applications such as packaging and insulation mainly due to their intrinsically high porosity, low relative density and associated mechanical and transport properties. Here hollow core spherical shells are prepared with walls made of a polyhedral silica nanofoam with open cells. A microemulsion film at the oil-water interface of oil droplets is used as a soft structural template for the condensation of soluble silica species. The microemulsion sets the length scale of the monodisperse silica nanofoam cells, and the emulsion droplets set the micron-scale dimensions of the polydisperse spherical shells. Porosity is achieved by removing the templates and oils, leaving pure low-density silica. This results in a hierarchically structured, highly porous shell foam material that packs into beds with a measured porosity of approximately 97.3%, well into the range of silica aerogels. Using a combination of electron microscopy, small-angle synchrotron X-ray diffraction and nitrogen physisorption, an accurate structural model for the nanofoam shells is constructed. The material is shown to be comprised of open-cell foams that are structurally analogous to dry polyhedral soap froths having minimal surface partitions, and Plateau boundaries. The primary polyhedral nanofoam cells are 30 nm in diameter connected by 7 nm cylindrical windows. These nanofoams form spherical monolithic shells with volume average mean diameter of 41 microns and shell thickness of 0.7 microns. Simple models for the thermal conductivity of these nanofoam shell materials are constructed that include accounting for the nanoscale effects on gaseous and solid thermal conductivity. These are compared to the measured value of 0.041 W m-1 K-1. These materials represent new structures in the family of self-assembled, highly porous silica materials and are potentially useful in packaging and insulation and other applications due to their light weight and/or intrinsically low thermal conductivity and associated mechanical and transport properties.

  • 9.
    Willgert, M.
    et al.
    KTH Royal Institute of Technology.
    Leijonmarck, Simon
    RISE, Swerea, Swerea SICOMP.
    Lindbergh, G.
    KTH Royal Institute of Technology.
    Malmström, E.
    KTH Royal Institute of Technology.
    Johansson, M.
    KTH Royal Institute of Technology.
    Cellulose nanofibril reinforced composite electrolytes for lithium ion battery applications2014In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 2, no 33, p. 13556-13564Article in journal (Refereed)
    Abstract [en]

    The present study describes the synthesis and characterization of a series of four composite electrolytes for lithium ion battery applications. The two-phase electrolytes are composed of a soft, ionic conductive poly(ethylene glycol) (PEG) matrix having stiff nanofibrillated cellulose (CNF) paper as reinforcement to provide mechanical integrity. The reinforcing CNF is modified in order to create covalent bonds between the phases which is particularly beneficial when swelling the composite with a liquid electrolyte to enhance the ionic conductivity. After swelling the composite polymer electrolyte, forming a gelled structure, values of ionic conductivity at 5 × 10-5 S cm-1 and an elastic modulus around 400 MPa at 25 °C are obtained. This journal is © the Partner Organisations 2014.

  • 10. Zhao, Y.
    et al.
    Sugunan, Abhilash
    RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Kemi Material och Ytor, Material och ytteknik. KTH Royal Institute of Technology, Sweden.
    Schmidt, T.
    Fornara, Andrea
    RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Kemi Material och Ytor, Material och ytteknik.
    Toprak, M. S.
    Muhammed, M.
    Relaxation is the key to longer life: Suppressed degradation of P3HT films on conductive substrates2014In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 2, no 33, p. 13270-13276Article in journal (Refereed)
    Abstract [en]

    Here we show the dependence of the degree of degradation of poly-3-hexylthiophene (P3HT) films on the conductivity of the supporting substrate. P3HT is widely used for organic solar cells and electronic devices because it allows simple, low cost fabrication and has potential for the fabrication of flexible devices. However, P3HT is known to have a relatively low photostability, and investigating the photodegradation mechanism is an active research field. We find that P3HT films on conductive substrates show significantly retarded degradation and retain their chemical and morphological features when compared to similar films on glass substrates. This 'substrate effect' in retarding the degradation of P3HT films is evident even upon prolonged exposure to air for up to five months.

  • 11.
    Zhao, Y.
    et al.
    KTH Royal Institute of Technology, Sweden.
    Sugunan, Abhilash
    RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Kemi Material och Ytor, Material och ytteknik.
    Schmidt, T.
    KTH Royal Institute of Technology, Sweden.
    Fornara, Andrea
    RISE, SP – Sveriges Tekniska Forskningsinstitut, SP Kemi Material och Ytor.
    Toprak, M. S.
    KTH Royal Institute of Technology, Sweden.
    Muhammed, M.
    KTH Royal Institute of Technology, Sweden.
    Relaxation is the key to longer life: Suppressed degradation of P3HT films on conductive substrates2014In: Journal of Materials Chemistry A, ISSN 2050-7488, Vol. 2, no 33, p. 13270-13276Article in journal (Refereed)
    Abstract [en]

    Here we show the dependence of the degree of degradation of poly-3-hexylthiophene (P3HT) films on the conductivity of the supporting substrate. P3HT is widely used for organic solar cells and electronic devices because it allows simple, low cost fabrication and has potential for the fabrication of flexible devices. However, P3HT is known to have a relatively low photostability, and investigating the photodegradation mechanism is an active research field. We find that P3HT films on conductive substrates show significantly retarded degradation and retain their chemical and morphological features when compared to similar films on glass substrates. This 'substrate effect' in retarding the degradation of P3HT films is evident even upon prolonged exposure to air for up to five months. 

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