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Spatially resolved investigation of complex multi-phase systems using μxRF, SEM-EDX and high resolution SyXRD
RISE, SP – Sveriges Tekniska Forskningsinstitut, CBI Betonginstitutet AB.ORCID iD: 0000-0003-1904-7426
2013 (English)In: Cement & Concrete Composites, ISSN 0958-9465, E-ISSN 1873-393X, Vol. 37, no 1, p. 241-245Article in journal (Refereed) Published
Abstract [en]

Spatially resolved analysis of complex multi-phase systems can be validated through different analytical methods. This study compares investigations by scanning electron microscopy coupled with energy dispersive X-ray fluorescence analysis and high resolution X-ray diffraction. The studied sulfate attacked cement paste containing fly ashes consists of different interacting crystalline and amorphous phases. The complementary methods revealed in detail changes in phase composition due to the chemical attack. The advantages and disadvantages of both methods are discussed and suggestions are given for combining them with additional methods to maximize the information content.

Place, publisher, year, edition, pages
2013. Vol. 37, no 1, p. 241-245
Keywords [en]
Cement paste, Comparison, Damaging mechanism, EDX-SEM, High resolution, Spatial investigations, Sulfate attack, SyXRD
National Category
Other Materials Engineering
Identifiers
URN: urn:nbn:se:ri:diva-2727Local ID: 3979OAI: oai:DiVA.org:ri-2727DiVA, id: diva2:960330
Available from: 2016-09-07 Created: 2016-09-07 Last updated: 2018-08-15Bibliographically approved

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http://www.sciencedirect.com/science/article/pii/S0958946512001825

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Mueller, Urs

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