This letter presents an experimental characterization technique for assessing the performance of terahertz harmonic mixers across a wide frequency range. The total signal transfer loss of three mixers was measured in both up- and down-conversion configurations, and the conversion loss was determined through the solution of a linear system of equations. The proposed method uses LO signals with a frequency offset to ensure single sideband measurements, thereby eliminating the need for image-reject filters. The three-mixer method was verified by measurements of millimeter-wave mixers, which matched the traditional characterization method using a calibrated source and power meter. Given this successful millimeter-wave demonstration, we characterized three WM-86 Schottky diode × 4-harmonic mixers from 2.2 to 3 THz. This technique presents a notable advantage for conducting broadband mixer characterizations, particularly in the terahertz frequency regime, which lacks tunable, wideband sources.