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On-line inductively coupled plasma-atomic emission spectroelectrochemistry: Real-time element-resolved electrochemistry
RISE Research Institutes of Sweden, Materials and Production, Corrosion. PSL University, France.
Sorbonne Université, France.
PSL University, France.
Sorbonne Université, France.
2023 (English)In: Current Opinion in Electrochemistry, E-ISSN 2451-9103, Vol. 41, article id 101350Article in journal (Refereed) Published
Abstract [en]

Electrochemical techniques are coupled with inductively coupled plasma (ICP) atomic emission spectrometry for in-line electrolyte analyses. In this way, direct measurement of the elemental dissolution rates in real-time or element-resolved electrochemistry can be carried out, complementary to conventional electrochemical measurements. This methodology can be used to obtain the element-specific reaction mechanisms under either spontaneous or polarized conditions up to part-per-billion level resolution with applications in diverse domains of corrosion science and interfacial reactivity. This review aims to summarize recent research activities using ICP coupled with other analytical techniques to answer specific questions on the mechanism of degradation of materials in aqueous or organic environments including the dissolution of metal oxides, catalysis, reaction stoichiometry, electrochemical kinetics, and photoelectrochemical reactivity.

Place, publisher, year, edition, pages
Elsevier B.V. , 2023. Vol. 41, article id 101350
Keywords [en]
Atomic emission spectroscopy; Corrosion; Dissolution; Electrolytes; Inductively coupled plasma; Reaction kinetics; Spectroelectrochemistry; AESEC; Atomic emission spectroelectrochemistries; Electrochemical techniques; Inductively coupled plasma atomic emission spectrometry; Inductively coupled plasma atomic emissions; Inductively coupled plasma atomic-emission spectrometries; Inductively coupled plasma-AES; Inductively coupled plasma-atomic emission spectrometry; Inductively-coupled plasma; Real- time; Catalysis
National Category
Materials Engineering
Identifiers
URN: urn:nbn:se:ri:diva-70646DOI: 10.1016/j.coelec.2023.101350Scopus ID: 2-s2.0-85166955317OAI: oai:DiVA.org:ri-70646DiVA, id: diva2:1830294
Note

This work was supported by Agence Nationale de Recherche (ANR) #ANR-22CE08-0015-01 (QUEENE) and #ANR-20-CE08-0031 (TAPAS 2020). The authors acknowledge financial support from Sorbonne Université and the Centre National de la Recherche Scientifique (CNRS), France.

Available from: 2024-01-22 Created: 2024-01-22 Last updated: 2024-02-12Bibliographically approved

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